ISO 6145-7:2018 Preview

Gas analysis -- Preparation of calibration gas mixtures using dynamic methods -- Part 7: Thermal mass-flow controllers

ISO 6145 is a series of documents dealing with various dynamic methods used for the preparation of calibration gas mixtures. This document specifies a method for continuous preparation of calibration gas mixtures, from nominally pure gases or gas mixtures by use of thermal mass-flow controllers. The method is applicable to preparation of mixtures of non-reacting species, i.e. those which do not react with any material of construction of the flow path in the thermal mass-flow controller or the ancillary equipment.

If this method is employed for preparation of calibration gas mixtures the optimum performance is as follows: the relative expanded measurement uncertainty U, obtained by multiplying the standard uncertainty by a coverage factor k = 2, is not greater than 2 %.

If pre-mixed gases are used instead of pure gases, mole fractions below 10−6 can be obtained. The measurement of mass flow is not absolute and the flow controller requires independent calibration.

The merits of the method are that a large quantity of the calibration gas mixture can be prepared on a continuous basis and that multi-component mixtures can be prepared as readily as binary mixtures if the appropriate number of thermal mass-flow controllers is utilized.

NOTE Gas blending systems, based upon thermal mass-flow controllers, and some including the facility of computerization and automatic control, are commercially available.


General information

  • Status :  Published
    Publication date : 2018-12
  • Edition : 3
    Number of pages : 14
  • :
    ISO/TC 158
    Analysis of gases
  • 71.040.40
    Chemical analysis

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